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1042 | 1043 | 1044 | 1045 | 1046 | 1036 | 1037 | 1038 | 1039 | 1040 | 1041 | 1034 | 1035 | 910 | 1032 | 935 | 1030 | 1031 | 1026 | 1027 | 1028 | 1029 | 1024 | 1025 | 1023 | 1021 | 1022 | 1018 | 1019 | 1020 | 1017 | 684 | 1016 | 1015 | 890 | 1014 | 1011 | 1012 | 1013 | 1010 | 1009 | 1008 | 1007 | 660 | 1006 | 690 | 1005 | 1002 | 1003 | 997 | 999 | 1000 | 1001 | 996 | 995 | 994 | 987 | 988 | 989 | 990 | 991 | 992 | 984 | 985 | 986 | 431 | 983 | 982 | 979 | 980 | 981 | 961 | 977 | 978 | 975 | 976 | 972 | 974 | 969 | 970 | 971 | 968 | 911 | 967 | 817 | 850 | 853 | 658 | 659 | 439 | 966 | 964 | 962 | 963 | 960 | 958 | 959 | 957 | 954 | 955 | 956 | 952 | 953 | 949 | 950 | 951 | 947 | 948 | 946 | 945 | 944 | 943 | 942 | 941 | 938 | 936 | 937 | 934 | 931 | 932 | 933 | 752 | 292 | 815 | 816 | 819 | 316 | 832 | 839 | 846 | 847 | 854 | 855 | 863 | 864 | 865 | 362 | 879 | 888 | 891 | 918 | 689 | 716 | 722 | 724 | 741 | 744 | 746 | 749 | 750 | 929 | 927 | 928 | 925 | 926 | 924 | 153 | 923 | 919 | 921 | 916 | 914 | 912 | 908 | 909 | 905 | 906 | 464 | 354 | 904 | 878 | 900 | 893 | 894 | 895 | 896 | 897 | 892 | 898 | 899 | 889 | 351 | 885 | 886 | 880 | 881 | 883 | 884 | 667 | 874 | 875 | 361 | 930 | 940 | 430 | 434 | 873 | 825 | 826 | 828 | 829 | 844 | 845 | 849 | 852 | 856 | 857 | 858 | 859 | 860 | 870 | 697 | 764 | 862 | 861 | 818 | 851 | 663 | 830 | 831 | 833 | 834 | 835 | 836 | 838 | 840 | 842 | 843 | 824 | 837 | 822 | 820 | 801 | 810 | 811 | 812 | 814 | 628 | 656 | 657 | 661 | 664 | 665 | 666 | 668 | 669 | 670 | 674 | 675 | 677 | 678 | 680 | 681 | 682 | 683 | 685 | 686 | 687 | 688 | 691 | 692 | 693 | 694 | 696 | 698 | 699 | 700 | 701 | 702 | 703 | 704 | 705 | 713 | 459 | 717 | 719 | 720 | 721 | 725 | 729 | 731 | 734 | 736 | 737 | 740 | 748 | 751 | 754 | 755 | 756 | 757 | 758 | 759 | 760 | 761 | 762 | 711 | 813 | 809 | 808 | 803 | 804 | 805 | 364 | 802 | 800 | 798 | 796 | 797 | 795 | 791 | 792 | 793 | 794 | 461 | 790 | 787 | 788 | 770 | 771 | 772 | 773 | 774 | 775 | 777 | 782 | 784 | 768 | 769 | 767 | 765 | 766 | 626 | 726 | 727 | 728 | 710 | 706 | 295 | 444 | 484 | 652 | 654 | 655 | 643 | 646 | 647 | 648 | 649 | 650 | 630 | 631 | 633 | 634 | 635 | 638 | 639 | 640 | 564 | 578 | 582 | 583 | 584 | 587 | 588 | 590 | 591 | 592 | 593 | 594 | 595 | 596 | 597 | 598 | 599 | 600 | 601 | 602 | 603 | 604 | 605 | 606 | 607 | 608 | 609 | 610 | 611 | 613 | 614 | 615 | 616 | 617 | 618 | 619 | 620 | 623 | 438 | 442 | 443 | 447 | 448 | 455 | 465 | 466 | 472 | 473 | 481 | 482 | 483 | 576 | 575 | 562 | 532 | 535 | 537 | 539 | 541 | 543 | 545 | 547 | 551 | 553 | 555 | 513 | 514 | 515 | 516 | 517 | 518 | 519 | 520 | 521 | 522 | 523 | 524 | 525 | 526 | 527 | 528 | 530 | 500 | 501 | 502 | 503 | 504 | 505 | 506 | 507 | 508 | 509 | 511 | 487 | 488 | 489 | 491 | 492 | 495 | 496 | 499 | 458 | 456 | 360 | 294 | 293 | 415 | 416 | 404 | 402 | 398 | 401 | 377 | 386 | 372 | 369 | 368 | 358 | 344 | 353 | 355 | 321 | 322 | 325 | 319 | 257 | 8 | 13 | 14 | 271 | 272 | 33 | 289 | 34 | 35 | 296 | 44 | 45 | 86 | 98 | 100 | 106 | 117 | 139 | 145 | 159 | 182 | 183 | 184 | 185 | 210 | 211 | 212 | 216 | 222 | 223 | 235 | 239 | 240 | 243 | 246 | 248 | 250 | 3587 | 3590 | 3160
Why so many bubbles in a fritted cone 6 glaze?
This is a cone 6 transparent fritted glaze (converted from a Gerstley Borate one). Its B2O3 content is high, sourced by Ferro Frit 3134. Bubbles like this plague many potters, many just keep trying new glazes until one works, or give up on never finding one.
The first obvious problem is the frit, it starts melting at 1350°F, while plenty of gases are still being generated. Such a bubble-trapper is a non-starter in an industrial continuous fast-fire kiln. They need late melters. But potters have flexible firing, so what could be done? The firing could be slowed down, leading up to 1350. It could be held at top temp, then either slow cooled or a drop-and-hold.
And the recipe?
Notice the big bubbles; they started as little ones that merged. Given enough time, big ones break at the surface, but only under the right conditions: Low enough melt viscosity and surface tension. That's not happening. Strangely, old recipes sourcing high boron from Gerstley Borate had surprisingly few problems with bubbles! Why? GB was its own fining agent. And its boron entered the melt much later than this frit. Plus, the melt developed unevenly, creating localized channels and variable viscosity zones for easier bubble escape. The larger bubbles could better move laterally by combinations of surface tension, layer thickness and temperature gradients, and downward movement that created shear. A frit is missing all of that.
Let's assume this glaze melt has high surface tension. It pulls liquid inward around each bubble, stabilizing them round and making rupture more difficult. But, if surface tension drops, even slightly, bubbles deform more easily and adjacent ones merge. What could help? Industrial technicians have found that surprisingly small changes can really help with bubble release.
-A small SiO2 or Al2O3 addition can delay surface sealing or change viscosity timing.
-Sourcing the CaO from wollastonite can help bubble coalescence and reduce melt surface tension.
-Zinc oxide often changes surface behavior more than expected. As little as 2% can alter the viscosity curve, surface tension and melt interface properties, weakening bubble walls and improving near-surface rupture.
-Although MgO stiffens the melt somewhat, it also changes bubble wall elasticity; even small additions can help bubbles merge better.
As usual with solutions found here, methodical testing is needed to find the best answer.
Related Pictures
Gerstley Borate vs Frit 3134 melt fluidity comparison
This picture has its own page with more detail, click here to see it.
This GLFL test compares the melting behavior of Gerstley Borate (GB) and Ferro Frit 3134 across a wide temperature range. Although both supply boron, they behave very differently because Gerstley Borate is a natural mineral blend while Frit 3134 is a premelted glass. Gerstley Borate shrinks dramatically to about half its original size by 1600°F, then suddenly becomes highly fluid between 1600–1650°F as reactive borate phases form and viscosity collapses. Frit 3134, by contrast, softens gradually, reflecting the progressive viscosity decline typical of a glass. It has no crystal decomposition or raw material phase changes, no sudden liberation of fluxes. It is softening while gases are still escaping (the GB was also foaming at 1650F).
So, if GB delivers boron through mineral breakdown and 3134 delivers it through viscosity-controlled glass softening, then why does a zero LOI frit have bubbles at 1700F? The dried ball is a compacted powder; it has plenty of voids. This melt begins extremely early, at 1350F, easily trapping air in the voids and gases generated by the binder holding the frit ball together. While bubbles have cleared this fluid melt by 1800F, a bubble-free glaze is much more challenging because there are more sources of decomposition gases and a stiffer, more viscous melt.
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